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This document is a compilation of practical work on the treatment of natural water and wastewater. Written in a clear and accessible manner, this manuscript is intended to assist those working in the quality control laboratories of water treatment plants for small and medium-sized enterprises, in the development of their day-to-day operations.This document details the procedures frequently performed on a routine basis in the laboratory of a water purification plant. It is aimed primarily at students on the M1 and M2 Environmental Chemistry Masters courses.